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Beilstein J. Org. Chem. 2014, 10, 1524–1535, doi:10.3762/bjoc.10.157
Graphical Abstract
Scheme 1: Synthesis of mannosylated trimers 5 and 9 using trimesic acid core transformed into propargylated (2...
Scheme 2: Divergent CuAAc “click reaction” between propargylated core 10 and azide 3 to afford 9-mer 12.
Scheme 3: Divergent CuAAc synthesis of “extended” 9-mer 17 using phloroglucinol (13) as core, bromoacylated T...
Scheme 4: Convergent synthesis of further “extended” 9-mer 21 using mannosylated bromoacyl dendron 18 transfo...
Scheme 5: Convergent assembly of 27-mer 23 using key propargylated scaffold precursors 10 and mannosylated az...
Figure 1: a) Decay of 1H signal for the nonavalent mannosylated compound 12 in D2O during the PFGSTE experime...